Sweetened Condensed Milk Quality Control: Sucrose and Total Solids

Sweetened Condensed Milk Quality Control: Sucrose and Total Solids

Sweetened condensed milk is a versatile ingredient used in a wide range of food applications. Its concentrated sweetness, smooth texture, and functional properties make it suitable for confectionery products such as candies and toffees, caramel-based products, chocolate bars and fillings, dessert sauces, prepared desserts, ice cream, fine bakery and pastry products, sweet spreads, cream fillings, and breakfast cereals. To ensure consistent product quality, shelf life, and regulatory compliance, manufacturers must closely monitor sucrose concentration and total solids (TS). Reliable analytical control is therefore essential throughout production. Polarimetry provides accurate laboratory verification, while inline refractometry enables continuous process monitoring. Used together, these complementary techniques help dairy manufacturers maintain batch consistency, improve production efficiency, and meet defined quality specifications. This application note explains how polarimetry and refractometry can be applied to determine sugar content, monitor total solids, and support sweetened condensed milk quality control.

How Is Sweetened Condensed Milk Produced?

The production of sweetened condensed milk involves several carefully controlled processing steps to achieve the required composition, product stability, and batch consistency. The process typically includes:
  • Standardization of milk fat and solids-not-fat (SNF) to establish a consistent composition of milk solids before processing
  • Heat treatment for microbial stabilization and product safety
  • Vacuum evaporation to remove water and increase the concentration of total milk solids
  • Addition of sucrose as dry sugar or syrup to achieve the required sugar concentration and preservation effect
  • Homogenization, if required, to improve product uniformity and stability
  • Controlled cooling and lactose crystallization to obtain the desired texture and mouthfeel
  • Filling and storage under hygienic conditions
During evaporation, water is removed under vacuum conditions, increasing the solids concentration of the milk. Sugar is subsequently added to achieve the required composition and preservation effect. Typical sweetened condensed milk products contain approximately 62.5–64.5% sugar. Because sugar acts as the primary preservation mechanism by increasing osmotic pressure, precise control of sugar concentration is essential for product stability and shelf life. At the same time, the concentration of solids must remain within specification to ensure consistent viscosity, texture, and processability.

Why Do Accurate Sucrose and Total Solids Measurements Matter?

Accurate monitoring of sucrose concentration and total solids is one of the most important quality-control measures in sweetened condensed milk production. Insufficient sugar concentration can reduce microbiological stability and shorten shelf life. Excessive sugar addition may negatively affect crystallization behavior, product texture, taste, and production costs. Variations in solids concentration can additionally result in:
  • Inconsistent viscosity
  • Uncontrolled lactose crystallization
  • Reduced product quality
  • Increased production costs
  • Process inefficiencies
  • Regulatory compliance challenges
To maintain consistent product quality, manufacturers require reliable analytical methods for laboratory verification as well as continuous process monitoring during production.

How Is Sucrose Determined by Polarimetry According to ISO 2911?

Sucrose is an optically active sugar that rotates polarized light. This property enables the highly accurate determination of sucrose concentration using polarimetry. International standards such as ISO 2911:2004 | IDF 35:2004 describe a standardized polarimetric method for determining sucrose content in sweetened condensed milk. The procedure involves clarification of the milk sample to remove proteins and fats, followed by optical rotation measurements before and after sucrose inversion. The sucrose concentration is then calculated from the change in optical rotation. Due to its accuracy, reproducibility, and standardization, polarimetry remains one of the most established analytical methods for sucrose analysis in dairy quality-control laboratories.

Which Laboratory Polarimeter Is Suitable for Sucrose Analysis in Condensed Milk?

The SCHMIDT + HAENSCH UniPol V digital polarimeter provides a reliable and highly accurate solution for determining sucrose concentration in sweetened condensed milk. As a laboratory instrument developed for the analysis of optically active substances in the food industry, it delivers precise and reproducible results that support quality assurance throughout the production process. The UniPol V is suitable for laboratory applications including:
  • Incoming raw-material inspection
  • Verification during production
  • Final-product quality control
  • Standardized sucrose determination
  • Regulatory compliance testing
  • Reliable measurements according to the established ISO 2911:2004-12 method
In dairy laboratories, the instrument is used to verify that the sucrose concentration meets product specifications after sugar addition and before product release. Its measurement accuracy and repeatability help ensure batch-to-batch consistency while providing dependable analytical data for documentation and regulatory compliance. Designed for routine quality control, the UniPol V combines precise measurement technology with straightforward operation. The intuitive touchscreen interface and Aquisys3 software allow users to manage measurement methods, enter sample information, and review results with minimal training. By combining analytical performance, ease of use, and robust laboratory design, the UniPol V is a suitable instrument for standardized sucrose analysis and reliable quality control in sweetened condensed milk production.

How Are Total Solids Monitored During Production?

While laboratory analysis verifies the quality of the finished product, efficient manufacturing requires continuous process monitoring directly in the production line. Inline measurement allows operators to observe concentration changes as they occur, eliminating delays associated with manual sampling and enabling immediate corrective action whenever process conditions deviate from specification. The refractive index of sweetened condensed milk is closely correlated with its total solids content. As water is removed during evaporation and sugar is added, the refractive index increases with the concentration of solids. Continuous inline refractive-index measurement therefore provides a reliable indicator of process concentration throughout production. Monitoring total solids at different stages of the process provides valuable information for both product quality and process efficiency. Measuring the solids content after milk standardization establishes the initial concentration, while measurement downstream of the evaporator verifies evaporation performance and confirms that the required solids level has been reached. Comparing these values enables manufacturers to calculate the required amount of sugar more accurately and achieve the target composition before crystallization and filling.

What Are the Benefits of Continuous Inline Concentration Monitoring?

  • Real-time process control
  • Immediate detection of concentration deviations
  • Optimization of evaporation efficiency
  • Improved sugar-dosing accuracy
  • Reduced manual sampling and laboratory workload
  • More stable production conditions
  • Consistent product quality
Because the measurement is performed continuously, operators can respond immediately to process fluctuations instead of waiting for laboratory results. This minimizes product variability, reduces waste, and contributes to a more economical and reproducible manufacturing process.

Which Inline Process Refractometer Is Suitable for Sweetened Condensed Milk Production?

The SCHMIDT + HAENSCH iPR FS inline process refractometer provides continuous, high-precision monitoring of total solids during sweetened condensed milk production. By measuring the refractive index directly in the process stream, the system supplies real-time concentration data for process optimization, automatic control, and quality assurance. Depending on the production layout, the iPR FS can be installed at several critical process points:
  • After milk standardization to verify the initial solids concentration
  • Downstream of the evaporator to monitor evaporation efficiency
  • Before crystallization, storage, or filling to confirm the target concentration
  • In a bypass installation for flexible integration into existing production lines
The measured values can be transmitted directly to the plant-control system via analog and digital interfaces. This enables automated regulation of evaporation, dosing, and other process parameters without interrupting production. Designed for hygienic food production, the EHEDG-certified iPR FS features a sanitary construction with smooth surfaces and hygienic process connections such as VariVent. The instrument supports both CIP and SIP cleaning procedures, allowing integration into existing cleaning cycles without removal from the process line. Its robust, maintenance-friendly design supports reliable long-term operation while minimizing downtime and maintenance effort. Together, these features make the iPR FS an effective solution for maintaining stable process conditions, optimizing resource utilization, and ensuring consistent product quality throughout sweetened condensed milk production.

Where Are Polarimetry and Inline Refractometry Used in Condensed Milk Production?

  • Sweetened condensed milk production
  • Sucrose content determination
  • Total solids monitoring
  • Evaporation process control
  • Sugar-dosing optimization
  • Final-product quality assurance
  • Dairy process monitoring
  • Regulatory compliance testing
Accurate quality control of sweetened condensed milk depends on two complementary analytical techniques. Polarimetry provides standardized laboratory determination of sucrose concentration according to the ISO 2911:2004-12 method, while inline refractometry continuously monitors total solids throughout production. Together, these technologies improve process control, product consistency, regulatory compliance, and manufacturing efficiency in modern dairy production.

Suggested Products

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